Utilize este identificador para referenciar este registo:
https://hdl.handle.net/1822/31839
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Campo DC | Valor | Idioma |
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dc.contributor.author | Rodríguez-Solana, Raquel | por |
dc.contributor.author | Salgado, José Manuel | por |
dc.contributor.author | Domínguez, José Manuel | por |
dc.contributor.author | Cortés-Diéguez, Sara | por |
dc.date.accessioned | 2014-12-11T12:25:07Z | - |
dc.date.available | 2014-12-11T12:25:07Z | - |
dc.date.issued | 2014-01-01 | - |
dc.identifier.citation | Rodríguez-Solana, Raquel; Salgado, José Manuel; Domínguez, José Manuel; Cortés-Diéguez, Sara, Estragole quantity optimization from fennel seeds by supercritical fluid extraction (carbon dioxide–methanol) using a Box–Behnken design. Characterization of fennel extracts. Industrial Crops and Products, 60, 186-192, 2014 | por |
dc.identifier.issn | 0926-6690 | por |
dc.identifier.uri | https://hdl.handle.net/1822/31839 | - |
dc.description.abstract | Oleoresin extraction from fennel seeds using a supercritical fluid extraction (SFE) was carried out. Box–Behnken experimental design was used to optimize the SFE variables: pressure (10, 17.5, and 25 MPa), temperature (313.15, 323.15, and 333.15 K) and time of extraction (1, 2.5, and 4 h). Different percentages of methanol (0, 3, and 6%) were also evaluated to improve the extraction of the corresponding volatile compounds. Besides volatile profile characterization of fennel seeds, the amount of estragole was determined (by gas chromatography-flame ionization detector (GC-FID)) due to its recent concern in being considered a potential carcinogen agent. The optimal values of SFE variables for methanol extracts were high levels of pressure (24 MPa), 333.15 K of temperature, 3.41 h of extraction time, and an intermediate value of methanol percentage (3%), obtaining an optimal value of 1320 ± 260 mg of estragole/kg dry plant. The volatile profile of the methanol extracts was evaluated by gas chromatography–mass spectrometry (GC–MS) obtaining mainly, terpenes, phenyl derivatives, and fatty acids. | por |
dc.description.sponsorship | We are grateful for the financial support of this work to the Spanish Ministry of Science and Innovation (project CTQ2011-28967), which has partial financial support from the FEDER funds of the European Union. Jose Manuel Salgado acknowledge the financial support from "Fundacao para a Ciencia e Tecnologia (FCT)" of Portugal through grant SFRH/BD/87953/2012. | por |
dc.language.iso | eng | por |
dc.publisher | Elsevier B.V. | por |
dc.rights | restrictedAccess | por |
dc.subject | Box–Behnken design | por |
dc.subject | Essential oils | por |
dc.subject | Estragole | por |
dc.subject | Fennel | por |
dc.subject | SFE | por |
dc.title | Estragole quantity optimization from fennel seeds by supercritical fluid extraction (carbon dioxide–methanol) using a Box–Behnken design : characterization of fennel extracts | por |
dc.type | article | - |
dc.peerreviewed | yes | por |
dc.comments | CEB18005 | por |
sdum.publicationstatus | published | por |
oaire.citationStartPage | 186 | por |
oaire.citationEndPage | 192 | por |
oaire.citationConferencePlace | Netherlands | - |
oaire.citationTitle | Industrial Crops and Products | por |
oaire.citationVolume | 60 | por |
dc.date.updated | 2014-11-28T17:47:48Z | - |
dc.identifier.eissn | 0926-6690 | - |
dc.identifier.doi | 10.1016/j.indcrop.2014.05.027 | por |
dc.subject.fos | Engenharia e Tecnologia::Biotecnologia Industrial | por |
dc.subject.wos | Science & Technology | por |
sdum.journal | Industrial Crops and Products | por |
Aparece nas coleções: | CEB - Publicações em Revistas/Séries Internacionais / Publications in International Journals/Series |
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document_18005_1.pdf Acesso restrito! | 1,15 MB | Adobe PDF | Ver/Abrir |